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Download Atom Probe Tomography: Analysis at the Atomic Level by M. K. Miller (auth.) PDF

By M. K. Miller (auth.)

The microanalytical means of atom probe tomography (APT) allows the spatial coordinates and elemental identities of the person atoms inside a small quantity to be decided with close to atomic answer. hence, atom probe tomography presents a method for buying atomic solution 3­ dimensional pictures of the solute distribution in the microstructures of fabrics. This monograph is designed to supply researchers and scholars the mandatory info to plot and experimentally behavior an atom probe tomography test. The options required to imagine and to investigate the ensuing three-d facts also are defined. The monograph is prepared into chapters each one masking a selected point of the procedure. the improvement of this strong microanalytical procedure from the origins offield ion microscopy in 1951, throughout the first third-dimensional atom probe prototype in-built 1986 to contemporary advertisement state of the art 3­ dimensional atom probe is documented in bankruptcy 1. A common advent to atom probe tomography is usually awarded in bankruptcy 1. a number of the the right way to fabricate appropriate needle-shaped specimens are offered in bankruptcy 2. The method to shape box ion pictures of the needle-shaped specimen is defined in bankruptcy three. additionally, the looks of microstructural beneficial properties and the knowledge that could be anticipated from box ion microscopy are summarized. a quick account of the theoretical foundation for methods of box ionization and box evaporation is usually included.

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B AI Overview and Historical Evolution 23 Plate VII. The solute distribution at the center of a 2-nm-diameter copper-enriched precipitate in a neutron-irradiated A55B pressure vessel steel. All atoms are shown. Enrichments of nickel, manganese, and silicon and a high level of iron are evident. Plate VIII. Atom map of a boron- and phosphorus-enriched film at a grain boundary in HA YNES® 242TM nickel base superalloy. The enrichment is evident at both y-y and Ni 2 Mo-y segments of the boundary. The molybdenum isoconcentration surface (16% Mo) also indicates molybdenum enrichment at the y-y segment ofthe boundary.

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